Optimization and Monitoring of Fast Reactions - InsightXpress from Bruker

Bruker
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InsightXpress enables the monitoring of fast reactions and rapid, screening of reaction conditions.

InsightXpress is the fastest of the Insight product line and ideal for rapid reaction optimization and reaction monitoring of fast reactions MR.

InsightXpress’s new stop-flow delivery pumps enable the screening of reaction conditions by NMR at an unprecedented speed. Using InsightXpress, Professor Lloyd-Jones and his colleagues at the University of Edinburgh gathered insights into the mechanism and kinetics of the Suzuki-Miyaura protodeboronation side reaction. They were able to monitor the decay of a reagent with half-life time of 1 second.

Key Features

Used when needed (Compatible with Open Access System)

Rapid and easy set-up

Low sample volumes (<600 μL/shot)

Unlimited shots

Variable ratios of reagents to explore different reaction conditions

Accurate temperature control (detailed kinetics studies)

Pre-magnetization of reagents for quantitative information

Precise timing using a trigger pulse

Reproducible with stable measured volume

Dead-time less than 150 ms, enabling the monitoring of fast reactions

Fast flow-rate injection (0.2 – 2 ml/s)

In-situ cleaning using dedicated solvent flush line

Compatible with all Bruker 5 mm Probes

Easy automatic optimization of NMR parameters

Intuitive software for data acquisition and analysis

Optimization and Monitoring of Fast Reactions - InsightXpress from Bruker